5FFG

Crystal structure of integrin alpha V beta 6 head

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-B
Synchrotron site	APS
Beamline	23-ID-B
Temperature [K]	100
Detector technology	CCD
Collection date	2013-11-06
Detector	MAR CCD 165 mm
Wavelength(s)	1.03318
Spacegroup name	C 1 2 1
Unit cell lengths	215.590, 77.560, 59.070
Unit cell angles	90.00, 101.46, 90.00

Refinement procedure

Resolution	46.987 - 2.250
R-factor	0.2084
Rwork	0.208
R-free	0.24640
RMSD bond length	0.007
RMSD bond angle	0.615
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.250
Number of reflections	44807
<I/σ(I)>	6.7
Completeness [%]	94.7
Redundancy	2.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	5% PEG3000 20% PEG200 0.1M MES