5DRB
Crystal structure of WNK1 in complex with WNK463
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-08-13 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 38.642, 57.670, 65.532 |
Unit cell angles | 90.00, 89.90, 90.00 |
Refinement procedure
Resolution | 65.530 - 1.650 |
R-factor | 0.1991 |
Rwork | 0.197 |
R-free | 0.24050 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.007 |
RMSD bond angle | 1.137 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.530 | 1.690 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.403 | |
Number of reflections | 34584 | |
<I/σ(I)> | 21.8 | 2.2 |
Completeness [%] | 99.4 | 98.1 |
Redundancy | 3.3 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 8 | 298 | 100 mM Tris, pH 8.0, 16% PEG550 MME, 4% PEG3350 |