5DJC
Fc Heterodimer Design 8.1 L368V/Y407A + T366V/K409F
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 31-ID |
Synchrotron site | APS |
Beamline | 31-ID |
Temperature [K] | 193 |
Detector technology | CCD |
Collection date | 2013-10-02 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.97931 |
Spacegroup name | P 1 |
Unit cell lengths | 60.242, 66.858, 72.771 |
Unit cell angles | 85.17, 80.71, 89.69 |
Refinement procedure
Resolution | 30.000 - 2.100 |
R-factor | 0.23192 |
Rwork | 0.229 |
R-free | 0.28465 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.177 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA (3.3.20) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0017) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 71.559 | 2.210 |
High resolution limit [Å] | 2.100 | 6.640 | 2.100 |
Rmerge | 0.044 | 0.264 | |
Rmeas | 0.092 | ||
Rpim | 0.065 | 0.023 | 0.630 |
Total number of observations | 123662 | 3491 | 17079 |
Number of reflections | 62804 | ||
<I/σ(I)> | 6.3 | 16.5 | 1.3 |
Completeness [%] | 96.4 | 88.1 | 95.2 |
Redundancy | 2 | 1.9 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 294 | 17% PEG 3350 + 100mM Ammonium Iodide |