5B7I
Cas3-AcrF3 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2016-03-19 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97791 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 97.304, 127.197, 218.455 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.600 |
R-factor | 0.2061 |
Rwork | 0.204 |
R-free | 0.24870 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.184 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 109.230 | 50.000 | 2.690 |
High resolution limit [Å] | 2.600 | 5.600 | 2.600 |
Rmerge | 0.117 | 0.056 | 0.816 |
Number of reflections | 41828 | ||
<I/σ(I)> | 6.9 | ||
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 13 | 12.7 | 12.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 15% PEG 3350, 100mM ammonium phosphate dibasic |