5AUY

Crystal structure of DAPK1 in complex with morin.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-5A
Synchrotron site	Photon Factory
Beamline	BL-5A
Temperature [K]	100
Detector technology	CCD
Collection date	2014-11-02
Detector	ADSC QUANTUM 315r
Wavelength(s)	1
Spacegroup name	P 21 21 21
Unit cell lengths	46.837, 62.210, 88.315
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	34.453 - 2.000
R-factor	0.2088
Rwork	0.207
R-free	0.24930
RMSD bond length	0.006
RMSD bond angle	0.962
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	PHENIX
Refinement software	PHENIX ((phenix.refine: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	34.500
High resolution limit [Å]	2.000
Number of reflections	17897
<I/σ(I)>	18.5
Completeness [%]	97.7
Redundancy	4.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	2 M ammonium sulfate, 0.1 M MES