5AGW
Bcl-2 alpha beta-1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-12 |
Detector | ADSC CCD |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 87.673, 87.673, 107.480 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.969 - 2.695 |
R-factor | 0.2051 |
Rwork | 0.202 |
R-free | 0.27190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | UNPUBLISHED BCL-2 BECLIN BH3 COMPLEX |
RMSD bond length | 0.009 |
RMSD bond angle | 1.274 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.970 | 2.790 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.100 | |
Number of reflections | 12081 | |
<I/σ(I)> | 18.29 | 1.08 |
Completeness [%] | 99.8 | 98.3 |
Redundancy | 13.4 | 9.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 0.02M CACL2, 0.1M MOPS PH7.0, 10% 2-PROPANOL |