5AFK

alpha7-AChBP in complex with lobeline and fragment 2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	CCD
Collection date	2013-04-02
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	85.695, 112.293, 144.305
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.841 - 2.381
R-factor	0.1701
Rwork	0.167
R-free	0.23000
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.008
RMSD bond angle	1.200
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	48.230
High resolution limit [Å]	2.381
Rmerge	0.070
Number of reflections	55979
<I/σ(I)>	17
Completeness [%]	99.7
Redundancy	5.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1