5AFJ

alpha7-AChBP in complex with lobeline and fragment 1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	CCD
Collection date	2012-11-10
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	85.203, 106.477, 140.989
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.383 - 2.200
R-factor	0.1715
Rwork	0.168
R-free	0.23290
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.007
RMSD bond angle	1.178
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	48.380
High resolution limit [Å]	2.220
Rmerge	0.060
Number of reflections	63044
<I/σ(I)>	12.2
Completeness [%]	98.8
Redundancy	3.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1