4ZZN
Human ERK2 in complex with an inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-07-01 |
| Detector | DECTRIS PILATUS |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 48.760, 69.700, 59.800 |
| Unit cell angles | 90.00, 108.71, 90.00 |
Refinement procedure
| Resolution | 28.570 - 1.330 |
| R-factor | 0.1747 |
| Rwork | 0.170 |
| R-free | 0.20230 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.060 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.6) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.570 | 1.370 |
| High resolution limit [Å] | 1.330 | 1.330 |
| Rmerge | 0.030 | 0.420 |
| Number of reflections | 61571 | |
| <I/σ(I)> | 20.6 | 1.9 |
| Completeness [%] | 70.9 | 5.8 |
| Redundancy | 3 | 1.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
