4ZS2
Structural complex of FTO/fluorescein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-01-12 |
Detector | Bruker AXIOM 200 |
Wavelength(s) | 0.9735 |
Spacegroup name | H 3 |
Unit cell lengths | 142.660, 142.660, 83.218 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.970 - 2.160 |
R-factor | 0.19921 |
Rwork | 0.198 |
R-free | 0.22854 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.154 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.150 |
Number of reflections | 33566 |
<I/σ(I)> | 23.2 |
Completeness [%] | 99.8 |
Redundancy | 7.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 100 mM sodium citrate (pH 5.8), 10% PEG 3350, 8% isopropanol |