4ZRP
TC:CD320
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2013-04-08 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 98.099, 98.099, 355.979 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.942 - 2.100 |
R-factor | 0.184 |
Rwork | 0.184 |
R-free | 0.20750 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.928 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.942 | |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.100 | 0.900 |
Number of reflections | 101389 | |
<I/σ(I)> | 12 | 1 |
Completeness [%] | 99.0 | 62.3 |
Redundancy | 4.8 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | Calcium Acetate, MES, PEG8000 |