4ZJC
Structures of the human OX1 orexin receptor bound to selective and dual antagonists
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-12-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.033 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 63.431, 66.466, 182.129 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.830 | 2.850 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.170 | |
Number of reflections | 18893 | |
<I/σ(I)> | 9.9 | 1.1 |
Completeness [%] | 99.9 | 99.5 |
Redundancy | 9.6 | 8.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 5.6 | 293 | 100 mM Sodium Citrate pH 5.6, 32% PEG 400, 200 mM Potossium |