4ZIV
Crystal structure of AcrB triple mutant in P21 space group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-04-14 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97625 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 152.278, 157.491, 219.155 |
Unit cell angles | 90.00, 92.74, 90.00 |
Refinement procedure
Resolution | 19.979 - 3.160 |
R-factor | 0.2732 |
Rwork | 0.270 |
R-free | 0.33540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2gif |
RMSD bond length | 0.014 |
RMSD bond angle | 1.801 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 109.750 | 3.330 |
High resolution limit [Å] | 3.160 | 3.160 |
Number of reflections | 176847 | |
<I/σ(I)> | 10.2 | 2.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 17.7 | 17.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 288 | 0.1 M MES pH 6.5, 0.2 M MgAc, 10% PEG 3350 |