4ZIE
Crystal Structure of core/latch dimer of Bax in complex with BimBH3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-08-22 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 95.440, 95.440, 36.353 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.970 - 1.797 |
R-factor | 0.1864 |
Rwork | 0.182 |
R-free | 0.22880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bd2 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.873 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.970 | 1.861 |
High resolution limit [Å] | 1.797 | 1.797 |
Rmerge | 0.064 | 1.184 |
Number of reflections | 16194 | |
<I/σ(I)> | 30.73 | 2.57 |
Completeness [%] | 99.9 | 99.43 |
Redundancy | 14.1 | 14.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 277 | PEG6000, bicine |