4ZI8
Structure of mouse clustered PcdhgC3 EC1-3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-12-12 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.123, 82.286, 237.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.170 - 1.698 |
R-factor | 0.2051 |
Rwork | 0.204 |
R-free | 0.23940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4zi9 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.170 | 1.759 |
High resolution limit [Å] | 1.698 | 1.698 |
Rmerge | 0.112 | 1.079 |
Number of reflections | 84132 | |
<I/σ(I)> | 5.38 | 0.53 |
Completeness [%] | 86.0 | 39 |
Redundancy | 3.3 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | seeded from 100 mM HEPES pH 7, 60% MPD, 100 mM CaCl2, into 100 mM HEPES pH 7, 20% MPD |