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4ZHQ

Crystal structure of Tubulin-Stathmin-TTL-MMAE Complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL17U
Synchrotron siteSSRF
BeamlineBL17U
Temperature [K]100
Detector technologyCCD
Collection date2014-11-19
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)0.97915
Spacegroup nameP 21 21 21
Unit cell lengths104.938, 156.809, 182.465
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.340 - 2.550
R-factor0.192
Rwork0.190
R-free0.24500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4tv8
Data reduction softwareSCALEPACK
Data scaling softwareSCALEPACK
Phasing softwareMLPHARE
Refinement softwareREFMAC (5.8.0049)
Data quality characteristics
 Overall
Low resolution limit [Å]39.340
High resolution limit [Å]2.550
Number of reflections98202
<I/σ(I)>13.7
Completeness [%]99.7
Redundancy7.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION6.72936% PEG, 5% glycerol, 0.1M MES, 30 mM CaCl2, 30 mM MgCl2

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