4YJQ
SYK kinase domain in complex with inhibitor GTC000224
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-04-28 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.933 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.402, 86.841, 40.236 |
Unit cell angles | 90.00, 93.42, 90.00 |
Refinement procedure
Resolution | 29.480 - 1.340 |
R-factor | 0.1622 |
Rwork | 0.161 |
R-free | 0.18350 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | In-house SYK model |
Data reduction software | MOSFLM (6.2.4) |
Data scaling software | SCALA (3.2.5) |
Refinement software | BUSTER (2.11.2) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.488 | 29.488 | 1.340 |
High resolution limit [Å] | 1.270 | 4.020 | 1.270 |
Rmerge | 0.050 | 0.035 | 0.497 |
Total number of observations | 261221 | 7953 | 37125 |
Number of reflections | 70711 | ||
<I/σ(I)> | 14.1 | 35.5 | 2.4 |
Completeness [%] | 99.6 | 98.4 | 99 |
Redundancy | 3.7 | 3.5 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 30% Jeffamine ED-2001, 10% Glycerol, 0.1M MES pH6.0, 5mM TCEP |