4YIZ
Crystal structure of engineered TgAMA1 lacking the DII loop in complex with an Eimeria tenella RON2D3 peptide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-04-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 265.928, 265.928, 94.160 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 59.500 - 2.200 |
R-factor | 0.188 |
Rwork | 0.187 |
R-free | 0.20700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ID 2Y8T |
RMSD bond length | 0.003 |
RMSD bond angle | 0.845 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.890 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.133 | 0.475 |
Number of reflections | 180412 | |
<I/σ(I)> | 6.6 | 3.4 |
Completeness [%] | 93.9 | 94.4 |
Redundancy | 4.3 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 291 | 0.1 M tri-sodium citrate pH 5.0 and 2.0 M ammonium sulfate |