4YH7
Crystal structure of PTPdelta ectodomain in complex with IL1RAPL1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-06-16 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 1.000 |
Spacegroup name | I 41 |
Unit cell lengths | 286.295, 286.295, 70.183 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.090 - 4.400 |
R-factor | 0.292 |
Rwork | 0.290 |
R-free | 0.32460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4YFC 2dju 2dlh |
RMSD bond length | 0.006 |
RMSD bond angle | 1.575 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | HKL-2000 |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 4.480 |
High resolution limit [Å] | 4.400 | 4.400 |
Rmerge | 0.424 | |
Number of reflections | 17618 | |
<I/σ(I)> | 17.7 | 2.2 |
Completeness [%] | 95.6 | 86 |
Redundancy | 4.2 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 15% PEG4000, 0.1 M MES |