4YF4
Crystal structure of Rv1284 in the presence of polycarpine at mildly acidic pH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-06-15 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.95382 |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 101.142, 154.345, 157.732 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.880 - 1.800 |
R-factor | 0.196 |
Rwork | 0.194 |
R-free | 0.24400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ylk |
RMSD bond length | 0.008 |
RMSD bond angle | 1.096 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.448 | |
Number of reflections | 105432 | |
<I/σ(I)> | 9.6 | 1.7 |
Completeness [%] | 98.8 | 92.4 |
Redundancy | 5.4 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 289 | 0.1 M K/Na tartrate, 0.1 M MES/NaOH, 10 mM polycarpine |