4YED
TcdA (CsdL)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-12-03 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 65.555, 97.117, 83.337 |
Unit cell angles | 90.00, 111.65, 90.00 |
Refinement procedure
Resolution | 32.766 - 1.900 |
R-factor | 0.16138 |
Rwork | 0.159 |
R-free | 0.20023 |
RMSD bond length | 0.018 |
RMSD bond angle | 1.903 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.900 |
Number of reflections | 76402 |
<I/σ(I)> | 26.6 |
Completeness [%] | 100.0 |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | 20% (w/v) PEG 3350 and 0.15 M DL-malic acid, pH 7.0 |