4Y0W
YeaZ from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-08-30 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.969 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 78.030, 198.443, 161.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.220 - 2.500 |
R-factor | 0.18187 |
Rwork | 0.178 |
R-free | 0.25024 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.354 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.220 | 2.640 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.827 | |
Number of reflections | 43728 | |
<I/σ(I)> | 13.7 | 2 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5.9 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 293 | 4M Sodium formate |