4XVB

Recombinant thaumatin in the presence of 1.5M PST at 293K

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL26B1
Synchrotron site	SPring-8
Beamline	BL26B1
Temperature [K]	293
Detector technology	CCD
Collection date	2014-10-12
Detector	RIGAKU SATURN A200
Wavelength(s)	1.00
Spacegroup name	P 41 21 2
Unit cell lengths	58.487, 58.487, 151.609
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.942 - 1.520
R-factor	0.1099
Rwork	0.109
R-free	0.12960
RMSD bond length	0.006
RMSD bond angle	1.100
Data scaling software	HKL-2000
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.550
High resolution limit [Å]	1.520	1.520
Rmerge	0.053	0.468
Number of reflections	41551
<I/σ(I)>	68.98	8.05
Completeness [%]	100.0	100
Redundancy	14.3	14.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	293	0.05 M ADA, 1.5M K-Na TARTRATE