4XHQ

Re-refinement the crystal structure of Dscam1 isoform 1.34, N-terminal four Ig domains

Experimental procedure

Spacegroup name	P 42 2 2
Unit cell lengths	99.172, 99.172, 163.991
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.834 - 1.948
R-factor	0.2047
Rwork	0.203
R-free	0.23320
RMSD bond length	0.018
RMSD bond angle	1.660
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Crystallization Conditions

crystal ID	method	pH	temperature	details
1				1.5 M AMMONIUM SULPHATE, 0.1 M HEPES PH 7.5