4X3T
Crystal structure of chromobox homolog 7 (CBX7) chromodomain with MS37452
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X6A |
| Synchrotron site | NSLS |
| Beamline | X6A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-11-06 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 1 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 54.004, 77.309, 66.842 |
| Unit cell angles | 90.00, 95.55, 90.00 |
Refinement procedure
| Resolution | 29.610 - 2.140 |
| R-factor | 0.20564 |
| Rwork | 0.203 |
| R-free | 0.25645 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.804 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 29.610 |
| High resolution limit [Å] | 2.140 |
| Number of reflections | 30060 |
| <I/σ(I)> | 26.9 |
| Completeness [%] | 99.0 |
| Redundancy | 2.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 290 | 0.05 M Zinc acetate, 20% PEG 3350 |
