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4X17

JC Mad-1 polyomavirus VP1 in complex with GD1b oligosaccharide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06DA
Synchrotron siteSLS
BeamlineX06DA
Temperature [K]100
Detector technologyPIXEL
Collection date2013-07-12
DetectorDECTRIS PILATUS 2M
Wavelength(s)1.0
Spacegroup nameC 1 2 1
Unit cell lengths149.740, 95.390, 128.880
Unit cell angles90.00, 110.40, 90.00
Refinement procedure
Resolution30.000 - 1.750
R-factor0.16097
Rwork0.160
R-free0.18149
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3nxd
RMSD bond length0.008
RMSD bond angle1.373
Data reduction softwareXDS
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0025)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.800
High resolution limit [Å]1.7501.750
Number of reflections170305
<I/σ(I)>15.52.4
Completeness [%]99.696.2
Redundancy5.75.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52930.1 M HEPES pH 7.5, 0.2 M KSCN, 12% PEG 3350

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