4X15
JC Mad-1 polyomavirus VP1 in complex with GM2 oligosaccharide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-08-12 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 150.490, 95.680, 129.720 |
Unit cell angles | 90.00, 110.30, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.110 |
R-factor | 0.17387 |
Rwork | 0.172 |
R-free | 0.20499 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3nxg |
RMSD bond length | 0.008 |
RMSD bond angle | 1.324 |
Data reduction software | XDS |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.160 |
High resolution limit [Å] | 2.110 | 2.110 |
Number of reflections | 99141 | |
<I/σ(I)> | 9.1 | 2.3 |
Completeness [%] | 99.3 | 99.3 |
Redundancy | 4.2 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M HEPES pH 7.5, 0.2 M KSCN, 12% PEG 3350 |