4WVM
Stonustoxin structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-24 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95659 |
Spacegroup name | P 43 |
Unit cell lengths | 107.911, 107.911, 244.345 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.150 - 3.100 |
R-factor | 0.2086 |
Rwork | 0.207 |
R-free | 0.23640 |
Structure solution method | SIRAS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.120 |
Data scaling software | XSCALE |
Phasing software | SHELXDE |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 38.150 |
High resolution limit [Å] | 3.100 |
Number of reflections | 50233 |
<I/σ(I)> | 11.72 |
Completeness [%] | 99.1 |
Redundancy | 4.59 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293.15 | 4.2 M NaCl |