4WU8

Structure of trPtNAP-NCP145

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	98.15
Detector technology	CCD
Collection date	2011-07-01
Detector	MAR CCD 165 mm
Wavelength(s)	1.07
Spacegroup name	P 21 21 21
Unit cell lengths	106.410, 109.630, 183.010
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	94.050 - 2.450
R-factor	0.215
Rwork	0.214
R-free	0.26300
RMSD bond length	0.008
RMSD bond angle	1.484
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	94.050	2.580
High resolution limit [Å]	2.450	2.450
Rmerge		0.492
Number of reflections	73961
<I/σ(I)>		1.6
Completeness [%]	93.4	68.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6	291.15	Manganese chloride, potassium chloride, potassium cacodylate