4WP5

Chaetomium thermophilum Mex67 NTF2-like domain complexed with Mtr2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Collection date	2012-01-31
Detector	PSI PILATUS 6M
Wavelength(s)	0.9686
Spacegroup name	P 32 2 1
Unit cell lengths	103.215, 103.215, 89.010
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.646 - 2.900
R-factor	0.2222
Rwork	0.221
R-free	0.25400
RMSD bond length	0.003
RMSD bond angle	0.701
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	44.700
High resolution limit [Å]	2.900
Number of reflections	12265
<I/σ(I)>	11.4
Redundancy	4.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	see publication for details