4WOB
Proteinase-K Pre-Surface Acoustic Wave
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | OTHER |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-05-07 |
| Detector | RIGAKU SATURN 944+ |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 67.840, 67.840, 106.721 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 31.505 - 1.900 |
| R-factor | 0.195 |
| Rwork | 0.188 |
| R-free | 0.25700 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.987 |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.900 |
| Number of reflections | 18606 |
| <I/σ(I)> | 13.1 |
| Completeness [%] | 91.0 |
| Redundancy | 6.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | 0.6 - 1.6 M Ammonium Sulfate, 0.1 M Tris, pH 8.0 |
