4WMU
STRUCTURE OF MBP-MCL1 BOUND TO ligand 2 AT 1.55A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-05-06 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 98.870, 135.900, 37.680 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.590 | |
High resolution limit [Å] | 1.550 | 6.930 | 1.550 |
Rmerge | 0.060 | 0.039 | 0.516 |
Rmeas | 0.066 | 0.044 | 0.567 |
Total number of observations | 455339 | ||
Number of reflections | 74736 | 959 | 5445 |
<I/σ(I)> | 17.61 | 36.84 | 3.42 |
Completeness [%] | 99.9 | 98.2 | 100 |
Redundancy | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | 10 MG/ML MBP-MCL1, 200MM MG FORMATE, 20% PEG3350, 1MM MALTOSE, 1MM ligand 2 |