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4WM6

High pressure protein crystallography of hen egg white lysozyme at 950 MPa

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron sitePhoton Factory
BeamlineAR-NW12A
Temperature [K]298
Detector technologyCCD
Collection date2013-02-12
DetectorADSC QUANTUM 210r
Wavelength(s)0.71
Spacegroup nameP 43
Unit cell lengths107.269, 107.269, 36.891
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution35.760 - 1.850
R-factor0.2035
Rwork0.199
R-free0.28445
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.015
RMSD bond angle1.728
Refinement softwareREFMAC (5.7.0032)
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]1.850
Number of reflections36471
<I/σ(I)>19.1
Completeness [%]99.3
Redundancy4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1BATCH MODE293Sodium chloride

226707

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