4WK0
Metal Ion and Ligand Binding of Integrin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-10-25 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97934 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.060, 117.070, 167.090 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.900 - 1.780 |
R-factor | 0.1872 |
Rwork | 0.186 |
R-free | 0.22310 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.086 |
Data scaling software | XDS |
Refinement software | PHENIX ((phenix.refine: dev_1760)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.900 |
High resolution limit [Å] | 1.780 |
Number of reflections | 113328 |
<I/σ(I)> | 7.17 |
Completeness [%] | 98.2 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 293 | 0.1 M HEPES 7.2, 16% PEG 6000 |