4WJK
Metal Ion and Ligand Binding of Integrin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-27 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97934 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.130, 116.750, 159.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.100 - 1.850 |
R-factor | 0.1922 |
Rwork | 0.191 |
R-free | 0.23770 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.063 |
Data scaling software | XDS |
Refinement software | PHENIX ((phenix.refine: dev_1760)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.103 |
High resolution limit [Å] | 1.850 |
Number of reflections | 82697 |
<I/σ(I)> | 6.55 |
Completeness [%] | 98.4 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 293 | 0.1 M HEPES 7.2, 16% PEG 6000 |