4WBG
Crystal structure of class C beta-lactamase Mox-1 covalently complexed with aztorenam
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-12-13 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.540, 59.250, 62.480 |
Unit cell angles | 90.00, 102.72, 90.00 |
Refinement procedure
Resolution | 29.720 - 1.900 |
R-factor | 0.17716 |
Rwork | 0.175 |
R-free | 0.21422 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.392 |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 60.950 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.079 |
Number of reflections | 27737 |
<I/σ(I)> | 7.75 |
Completeness [%] | 99.4 |
Redundancy | 6.77 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 289 | PEG8000, cacodylate, zinc acetate |