4V7Y
Structure of the Thermus thermophilus 70S ribosome complexed with azithromycin.
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 24-ID-E |
| Synchrotron site | APS |
| Beamline | 24-ID-E |
| Temperature [K] | 100 |
| Wavelength(s) | 0.979180 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 210.220, 450.250, 623.810 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.803 - 3.000 |
| Rwork | 0.235 |
| R-free | 0.26930 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.115 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.250 | 3.080 |
| High resolution limit [Å] | 3.000 | 3.160 | 3.000 |
| Rmerge | 0.238 | 0.922 | 1.790 |
| Number of reflections | 1161538 | ||
| <I/σ(I)> | 6.89 | 1.68 | 0.85 |
| Completeness [%] | 99.5 | 99.7 | 95.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
