4V59
Crystal structure of fatty acid synthase complexed with nadp+ from thermomyces lanuginosus at 3.1 angstrom resolution.
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 215.780, 412.670, 220.900 |
| Unit cell angles | 90.00, 111.57, 90.00 |
Refinement procedure
| Resolution | 12.000 - 3.100 |
| Rwork | 0.270 |
| R-free | 0.30000 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 3.280 |
| High resolution limit [Å] | 3.100 | 3.100 |
| Rmerge | 0.240 | 0.800 |
| Number of reflections | 645016 | |
| <I/σ(I)> | 6.5 | 2.3 |
| Completeness [%] | 99.7 | 98.4 |
| Redundancy | 7.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6 | pH 6.0 |
