4V58

Crystal structure of fatty acid synthase from thermomyces lanuginosus at 3.1 angstrom resolution.

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 1 21 1
Unit cell lengths	216.370, 414.430, 221.510
Unit cell angles	90.00, 111.65, 90.00

Refinement procedure

Resolution	12.000 - 3.100
Rwork	0.290
R-free	0.32000
Structure solution method	OTHER
Starting model (for MR)	NONE
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	100.000	3.270
High resolution limit [Å]	3.100	3.100
Rmerge	0.160	0.630
Number of reflections	629509
<I/σ(I)>	5.7	1.8
Completeness [%]	96.4	93.8
Redundancy	3.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6		pH 6.0