4V58
Crystal structure of fatty acid synthase from thermomyces lanuginosus at 3.1 angstrom resolution.
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 216.370, 414.430, 221.510 |
Unit cell angles | 90.00, 111.65, 90.00 |
Refinement procedure
Resolution | 12.000 - 3.100 |
Rwork | 0.290 |
R-free | 0.32000 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 3.270 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.160 | 0.630 |
Number of reflections | 629509 | |
<I/σ(I)> | 5.7 | 1.8 |
Completeness [%] | 96.4 | 93.8 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | pH 6.0 |