4V42

Crystal structure of the ribosome at 5.5 A resolution.

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 4
Spacegroup name	I 4 2 2
Unit cell lengths	507.200, 507.200, 803.660
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	250.000 - 5.500
Structure solution method	MAD
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CCP4

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	250.000	5.700
High resolution limit [Å]	5.000	5.500
Rmerge		0.308
Number of reflections	209044
<I/σ(I)>		3.3
Completeness [%]	95.3	95
Redundancy	2.8	2.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1