4V3K
RNF38-UbcH5B-UB complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-07-01 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 139.620, 139.620, 70.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.905 - 2.040 |
R-factor | 0.1829 |
Rwork | 0.181 |
R-free | 0.22340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 3ZNI AND 1X4J |
RMSD bond length | 0.008 |
RMSD bond angle | 1.184 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.900 | 2.090 |
High resolution limit [Å] | 2.040 | 2.040 |
Rmerge | 0.120 | 0.820 |
Number of reflections | 44936 | |
<I/σ(I)> | 18.4 | 3.8 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 9.4 | 9.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 50 MM TRIS-HCL, PH 8.5 AND 2.3 M AMMONIUM SULFATE |