4V0X
The crystal structure of mouse PP1G in complex with truncated human PPP1R15B (631-684)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-01-17 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 67.540, 67.540, 158.010 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 51.337 - 1.850 |
R-factor | 0.1789 |
Rwork | 0.177 |
R-free | 0.22220 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | THE CRYSTAL STRUCTURE OF MOUSE PP1G IN COMPLEX WITH TRUNCATED HUMAN PPP1R15B INCLUDING 631-660 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.221 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | CCP4I |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.340 | 1.890 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.090 | 0.980 |
Number of reflections | 32078 | |
<I/σ(I)> | 9.7 | 1.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.8 | 8.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 2.0 M SODIUM MALONATE, PH6.0 |