4V04
FGFR1 in complex with ponatinib.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | RIGAKU CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 207.255, 58.090, 65.231 |
Unit cell angles | 90.00, 107.38, 90.00 |
Refinement procedure
Resolution | 21.370 - 2.120 |
R-factor | 0.1881 |
Rwork | 0.186 |
R-free | 0.22800 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.050 |
Refinement software | BUSTER (2.11.5) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 98.000 |
High resolution limit [Å] | 2.120 |
Rmerge | 0.040 |
Number of reflections | 41149 |
Completeness [%] | 97.0 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 18-20% (W/V) PEG 8000, 200MM AMMONIUM SULPHATE, 100MM PCTP PH6.75, 20% (V/V) ETHYLENE GLYCOL |