4UYZ
STRUCTURE OF THE WNT DEACYLASE NOTUM - CRYSTAL FORM II - 2.8A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Collection date | 2012-01-28 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 60.829, 193.880, 75.717 |
Unit cell angles | 90.00, 91.88, 90.00 |
Refinement procedure
Resolution | 96.940 - 2.800 |
R-factor | 0.24899 |
Rwork | 0.248 |
R-free | 0.29294 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 1.267 |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 58.000 |
High resolution limit [Å] | 2.800 |
Rmerge | 0.160 |
Number of reflections | 38300 |
<I/σ(I)> | 6.6 |
Completeness [%] | 89.1 |
Redundancy | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | pH 6.0 |