4UWN
Lysozyme soaked with a ruthenium based CORM with a methione oxide ligand (complex 6b)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-06-30 |
Detector | ADSC CCD |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.930, 79.930, 36.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.520 - 1.670 |
R-factor | 0.16794 |
Rwork | 0.166 |
R-free | 0.21153 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 193l |
RMSD bond length | 0.013 |
RMSD bond angle | 1.533 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.520 | 1.760 |
High resolution limit [Å] | 1.670 | 1.670 |
Rmerge | 0.060 | |
Number of reflections | 14435 | |
Completeness [%] | 99.9 | 100 |
Redundancy | 7 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 2-10% (M/V) NACL IN 0.1 M ACETATE BUFFER PH 4.5. PROTEIN STOCK CONCENTRATION OF 50 MG/ML. HANGING DROP VAPOR DIFFUSION METHOD, 293K |