4UVC
LSD1(KDM1A)-CoREST in complex with 1-Phenyl-Tranylcypromine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 118.960, 179.090, 234.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 68.530 - 3.100 |
R-factor | 0.21094 |
Rwork | 0.210 |
R-free | 0.24114 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v1d |
RMSD bond length | 0.006 |
RMSD bond angle | 1.097 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0027) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 3.270 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.190 | 1.320 |
Number of reflections | 45854 | |
<I/σ(I)> | 9 | 1.2 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 6.1 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.5 |