4UV8
LSD1(KDM1A)-CoREST in complex with 1-Benzyl-Tranylcypromine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 119.850, 179.210, 235.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.960 - 2.800 |
R-factor | 0.22579 |
Rwork | 0.226 |
R-free | 0.23700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v1d |
RMSD bond length | 0.005 |
RMSD bond angle | 0.913 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0027) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.080 | 0.830 |
Number of reflections | 62089 | |
<I/σ(I)> | 12.5 | 1.5 |
Completeness [%] | 99.3 | 98.4 |
Redundancy | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.5 |