4URK
PI3Kg in complex with AZD6482
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Collection date | 2005-02-11 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 143.179, 67.521, 106.167 |
Unit cell angles | 90.00, 95.71, 90.00 |
Refinement procedure
Resolution | 40.800 - 2.900 |
R-factor | 0.2535 |
Rwork | 0.250 |
R-free | 0.30900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | WWPDB ENTRY 1E8Y |
RMSD bond length | 0.009 |
RMSD bond angle | 1.110 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.800 | 2.980 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.060 | 0.380 |
Number of reflections | 21692 | |
<I/σ(I)> | 8.6 | 2 |
Completeness [%] | 96.0 | 96 |
Redundancy | 2.6 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 20% PEG3350, 0.1M HEPES (PH 7.5), 5% AMSO4, 10MM DTT |