4UO7
Structure of the A_Canine_Colorado_17864_06 H3 haemagglutinin in complex with 6SO4 Sialyl Lewis X
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 167.306, 348.485, 95.813 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 174.240 - 3.000 |
| R-factor | 0.23516 |
| Rwork | 0.233 |
| R-free | 0.27595 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4uo4 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.229 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.720 | 3.210 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.100 | 0.470 |
| Number of reflections | 53827 | |
| <I/σ(I)> | 10.4 | 2.3 |
| Completeness [%] | 95.6 | 95.6 |
| Redundancy | 3.3 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
