4UO6
Structure of the A_Canine_Colorado_17864_06 H3 haemagglutinin in complex with Sialyl Lewis X
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 2M |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 96.926, 96.926, 349.576 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 174.790 - 2.900 |
| R-factor | 0.19001 |
| Rwork | 0.188 |
| R-free | 0.23451 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4uo4 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.249 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.460 | 3.060 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rmerge | 0.100 | 0.650 |
| Number of reflections | 22519 | |
| <I/σ(I)> | 17.6 | 2.3 |
| Completeness [%] | 99.6 | 99.6 |
| Redundancy | 8.9 | 9.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
